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4,4′,4′′-Trimethyl-2,2′:6′,2′′-terpyridine by Oxidative Coupling of 4‑Picoline
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02264nam^^22003613a^4500
001
AA00002428_00001
005
20210621180009.0
006
m^^^^^o^^^^^^^^^^^
007
cr^^n^---ma^mp
008
210621n^^^^^^^^xx^^^^^^s^^^^^^^^^^^eng^d
245
00
|a
4,4′,4′′-Trimethyl-2,2′:6′,2′′-terpyridine by Oxidative Coupling of 4‑Picoline
|h
[electronic resource].
260
|a
Edison, NJ :
|b
Middlesex College,
|c
2015 December 20.
490
|a
Student Symposium 2015.
520
3
|a
My research is based on an article published in The Journal of Organic Chemistry(J. Org. Chem. 2014, 79, 10624-10628)about a new innovative method of synthesizing terpyridine. The proposed new method is a one-step reaction that takes up to 7 days, followed by sublimation to purify the product. My input to this project was to try and find a different way to purify the product without using sublimation. So far I have managed to actually synthesize the desired products,come up with a desired solvent system for thin layer chromatography(TLC), column chromatography and prep-thin layer chromatography(Prep-TLC). I have also analyzedmy results using nuclear magnetic resonance(NMR) spectroscopyand high performance liquid chromatography (HPLC). I have also found a promising method to crystalizing the product.
533
|a
Electronic reproduction.
|c
Middlesex County College Institution,
|d
2021.
|f
(Middlesex County College)
|n
Mode of access: World Wide Web.
|n
System requirements: Internet connectivity; Web browser software.
535
1
|a
Middlesex County College Institution.
648
|a
2015-2016
|y
Academic Year 2015-2016.
650
0
|a
College students -- poster presentations.
650
0
|a
Student Works -- Natural Sciences -- poster presentations.
650
0
|a
Chemistry.
650
0
|a
Student works -- Natural Sciences -- academic theses.
650
|a
Middlesex College (Edison, NJ) -- Student works.
650
0
|a
Middlesex County College (Edison, NJ).
700
1
|a
Odzelashvili, Amiran,
|e
author, primary.
700
1
|a
Ghosh, Phalguni,
|e
advisor.
700
|a
Middlesex College, Department of Natural Sciences.
|4
spn
830
0
|a
Middlesex County College.
830
0
|a
Student Symposium.
830
0
|a
Student Works.
852
|a
MCC
|c
Student Symposium
856
40
|u
http://middlesexcc.sobeklibrary.com/AA00002428/00001
|y
Electronic Resource
992
04
|a
https:/digital.middlesexcc.edu/content/AA/00/00/24/28/00001/Thesis-Amiran Odzelashvili- Award wining Research - 12-20-2015thm.jpg
997
|a
Student Symposium
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